By Willemse J. A.
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Additional info for Carbon Monoxide as Reagent in the Formulation of Aromatic Compounds
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Acad. Sci. , 10, 1956, 233. , Angew. , Int. Ed. , 3, 1964, 132. , J. Chem. Soc. Chem. , 1979, 1180. , J. Org. , 49, 1984, 3963-3966. , 67, 1934, 370-373. , J. Gen. Chem. USSR, 16, 1946, 203. , J. Am. Chem. , 82, 1960, 2380. , Synthesis, 1973, 487-488. , Angew. Chem. Int. Ed. , 18, 1979, 614. , Compt. , 128, 1899, 1460. , J. Org. , 23, 1958, 727-729. , US. Patent 2135709, 1938. , J. Am. Chem. , 61, 1939, 3355-3359. , J. Am. Chem. , 82, 1960, 2380. , Chem. , 113, 1980, 2086-2099. , 96, 1963, 308.
Our attempts to isolate the superacid from these solutions via reduced pressure distillation were not successful and is indicative of the strong complex formation between the acid and the oxygen moiety of ether and water. 3. 1 Phenol and Anisole Although a plethora of reagents does exist for the formylation of aromatic hydrocarbons with CO as reagent, this reaction generally fails with phenolic substrates. However, only a single patent196 by Hoechst Aktiengesellschaft and two papers by Takezaki,197,198 which utilise HF/BF3 as catalyst, describe the formation of phenolic aldehydes by formylation with CO.